Propellants Manufacture, Hazards, and Testing by Gould R.F. (ed.)

By Gould R.F. (ed.)

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By Gould R.F. (ed.)

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The 1st NATO technological know-how discussion board used to be held in Biarritz in September 1990. This Taormina convention is the second one in a sequence that we want to be an extended one and that i think that it has equalled the good fortune of its predecessor. In constructing those conferences the NATO technological know-how Committee desired to assemble top specialists to study fields of sturdy current curiosity.

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The method involves the selective extraction of the compound into ether, hydrolysis tb the 2-amino-5-chlorobenzophenone and subsequent determination by gas-liquid chromatography. The GLC of unhydrolyzed chlordiazepoxide has been reported by Martin and Street2' using acid-washed chromosorb W coated with dimethyldichlorosilane. The reported column temperature for chlordiazepoxide was 245'C. 3) B Ch 1o rofom :me th ano1 (1O:l) B Ethylacetate:ethanol (9:l) B Benzene:dioxane: 28% ammonium hydroxide A Acetone: cyclohexane: ethanol (4:4:2) A Benzene:acetone (4:l) A Methano1:acetone: ammonium hydroxide (50 :50:1) A Benzene:ethanol:25% ammonium hydroxide (50:10:5) A Adsorbant: I 48 48 29 57 46 - Detection w2 54 "254 "254 "2 54 w254 w254 38 Reference 22 22 22 22 22 23 w254 23 Dragendorff Reagent 24 27 II 24 41 11 24 78 64 A.

Personal Communication. 9. , Personal Communication. 10. MacMullan, E . A . , Personal Communication. 51 G, 523 (1967). CYCLOSERINE J. Lamb 53 J. W. LAMB C OI; 1. 2. 3. 4. 5. 6. 7. 53 P h o t o m e t r i c S y s t e m References - 54 CYCLOSERINE 1. 1 Name, F o r z u l a , M o l e c u l a r W e i g h t Cycloserine is ~-4-amino-3isoxazolidone. ihite t o s l i g h t l y yellow, p r a c t i c a l l y o d o r l e s s c r y s t a l l i n e powder. 2. 1 I n f r a r e d Spectrum ':he i n f r a r e d spectrum of cycloserine p r e s e n t e d i n F i g .

A. , Krol, G. , J . PharmacoZ. Exp. , 148, 339 (1965). , J. Pharm. S c i . , 55, 1358 (1966). , Personal Communication. 36 CHLORDIAZEPOXI DE 21. 22. 23. 24. 25. 26. National FomuZary XIII, 148-149 ( 1 9 7 0 ) . R o e t e r , E. , Z e i t , f. Anal. , (1969). D. 18, 529 ( 1 9 6 8 ) . , E , 45 and S m i t h , S . J . , Arneim. , Tomoda, M. Kyoritsu Yakka Daigaku Kenkyv Neppo, 18 ( 1 9 6 5 ) . Thomas, J . J . and P y r o n , L. J . , J . P h m . , 10, 19, 481 (1964). e t a l . , (1963). , J . Chrom.

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