By James Yurko, Antoine Allanore, Laura Bartlett, Jonghyun Lee, Lifeng Zhang, Gabriella Tranell, Yulia Meteleva-Fischer, Shadia Ikhmayies, Arief Budiman, Prabhat Tripathy, Guy Fredrickson
EPD Congress is an annual assortment that addresses extraction and processing metallurgy. The papers during this booklet are drawn from symposia held on the 2015 Annual assembly of The Minerals, Metals & fabrics Society. The 2015 variation comprises papers from the next symposia: •Materials Processing basics •Solar cellphone Silicon •High-Temperature Electrochemistry II
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The tungsten wire was polished successively with 22 72 increasingly finer grades of emery paper and then rinsed well for several times with ethanol and distilled water and then dried in air. All the electrochemical experiments were performed using EG&G PARC model 273A Potentiostat/Galvanostat under an Ar atmosphere. Electrochemical experiments were performed using a three-electrode cell system . 25 cm2, Alfa Aesar) as cathode electrode. The as-deposited sample was washed using anhydrous ethanol to remove any salt contaminants that adhere to the cathode surface.
I. -W. Sun, “Electrodeposition behavior of cadmium telluride from 1-ethyl-3methylimidazolium chloride tetrafluoroborate ionic liquid,” J. Appl. , 34 (2004), 1057-1063. 13. R. T. C. D. Long, “Electrodeposition of Cobalt-Aluminum Alloys from Room Temperature Chloroaluminate Molten Salt,” J. Electrochem. , 143 (9) (1996), 2747-2758. 14. R. T. , “Microelectrode Evaluation of Transition Metal-Aluminum Alloy Electrodepositions in Chloroaluminate Ionic Liquids,” J. Electrochem. , 145 (5) (1998), 1598-1607.
20 M of Co(BF4)2 at 353 K. Chronoamperometric experiments shows that the electrodeposition of cobalt is a 3D progressive nucleation process under diffusion control. 6 × 10-8 cm2s-1) from cyclic voltammetry. A dense and compact electrodeposit of cobalt was obtained under the experimental conditions. EDS and XRD results show that the electrodeposit is mainly composed of cobalt metal. Acknowledgements The author (Min Li) is thankful for the award of scholarship by China Scholarship Council (CSC) to pursue study as a visiting student at the Department of Metallurgical and Materials Engineering, The University of Alabama, Tuscaloosa, Alabama, United States of America.