Analytical Profiles of Drug Substances, Vol. 1 by FLOREY KLAUS

By FLOREY KLAUS

Profiles of Drug components, Excipients and comparable method vol 1. content material: entrance disguise; Analytical Profiles of Drug ingredients, quantity 1; Copyright web page; Contents; AFFILIATIONS OF EDITORS, participants, AND REVIEWERS; FOREWORD; PREFACE; bankruptcy 1. Acetohexamide; bankruptcy 2. Chlordiazepoxide; bankruptcy three. Chlordiazepoxide Hydrochloride; bankruptcy four. Cycloserine; bankruptcy five. Cyclothiazide; bankruptcy 6. Diazepam; bankruptcy 7. Erythromycin Estolate; bankruptcy eight. Halothane; bankruptcy nine. Levarterenol Bitartrate; bankruptcy 10. Meperidine Hydrochloride; bankruptcy eleven. Meprobamate; bankruptcy 12. Nortriptyline Hydrochloride; bankruptcy thirteen. Potassium Phenoxymethyl Penicillin. bankruptcy 14. Propoxyphene HydrochlorideChapter 15. Sodium Cephalothin; bankruptcy sixteen. Sodium Secobarbital; bankruptcy 17. Triamcinolone; bankruptcy 18. Triamcinolone Acetonide; bankruptcy 19. Triamcinolone Diacetate; bankruptcy 20. Vinblastine Sulfate; bankruptcy 21. Vincristine Sulfate. summary: Profiles of Drug ingredients, Excipients and comparable method vol 1

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By FLOREY KLAUS

Profiles of Drug components, Excipients and comparable method vol 1. content material: entrance disguise; Analytical Profiles of Drug ingredients, quantity 1; Copyright web page; Contents; AFFILIATIONS OF EDITORS, participants, AND REVIEWERS; FOREWORD; PREFACE; bankruptcy 1. Acetohexamide; bankruptcy 2. Chlordiazepoxide; bankruptcy three. Chlordiazepoxide Hydrochloride; bankruptcy four. Cycloserine; bankruptcy five. Cyclothiazide; bankruptcy 6. Diazepam; bankruptcy 7. Erythromycin Estolate; bankruptcy eight. Halothane; bankruptcy nine. Levarterenol Bitartrate; bankruptcy 10. Meperidine Hydrochloride; bankruptcy eleven. Meprobamate; bankruptcy 12. Nortriptyline Hydrochloride; bankruptcy thirteen. Potassium Phenoxymethyl Penicillin. bankruptcy 14. Propoxyphene HydrochlorideChapter 15. Sodium Cephalothin; bankruptcy sixteen. Sodium Secobarbital; bankruptcy 17. Triamcinolone; bankruptcy 18. Triamcinolone Acetonide; bankruptcy 19. Triamcinolone Diacetate; bankruptcy 20. Vinblastine Sulfate; bankruptcy 21. Vincristine Sulfate. summary: Profiles of Drug ingredients, Excipients and comparable method vol 1

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The method involves the selective extraction of the compound into ether, hydrolysis tb the 2-amino-5-chlorobenzophenone and subsequent determination by gas-liquid chromatography. The GLC of unhydrolyzed chlordiazepoxide has been reported by Martin and Street2' using acid-washed chromosorb W coated with dimethyldichlorosilane. The reported column temperature for chlordiazepoxide was 245'C. 3) B Ch 1o rofom :me th ano1 (1O:l) B Ethylacetate:ethanol (9:l) B Benzene:dioxane: 28% ammonium hydroxide A Acetone: cyclohexane: ethanol (4:4:2) A Benzene:acetone (4:l) A Methano1:acetone: ammonium hydroxide (50 :50:1) A Benzene:ethanol:25% ammonium hydroxide (50:10:5) A Adsorbant: I 48 48 29 57 46 - Detection w2 54 "254 "254 "2 54 w254 w254 38 Reference 22 22 22 22 22 23 w254 23 Dragendorff Reagent 24 27 II 24 41 11 24 78 64 A.

Personal Communication. 9. , Personal Communication. 10. MacMullan, E . A . , Personal Communication. 51 G, 523 (1967). CYCLOSERINE J. Lamb 53 J. W. LAMB C OI; 1. 2. 3. 4. 5. 6. 7. 53 P h o t o m e t r i c S y s t e m References - 54 CYCLOSERINE 1. 1 Name, F o r z u l a , M o l e c u l a r W e i g h t Cycloserine is ~-4-amino-3isoxazolidone. ihite t o s l i g h t l y yellow, p r a c t i c a l l y o d o r l e s s c r y s t a l l i n e powder. 2. 1 I n f r a r e d Spectrum ':he i n f r a r e d spectrum of cycloserine p r e s e n t e d i n F i g .

A. , Krol, G. , J . PharmacoZ. Exp. , 148, 339 (1965). , J. Pharm. S c i . , 55, 1358 (1966). , Personal Communication. 36 CHLORDIAZEPOXI DE 21. 22. 23. 24. 25. 26. National FomuZary XIII, 148-149 ( 1 9 7 0 ) . R o e t e r , E. , Z e i t , f. Anal. , (1969). D. 18, 529 ( 1 9 6 8 ) . , E , 45 and S m i t h , S . J . , Arneim. , Tomoda, M. Kyoritsu Yakka Daigaku Kenkyv Neppo, 18 ( 1 9 6 5 ) . Thomas, J . J . and P y r o n , L. J . , J . P h m . , 10, 19, 481 (1964). e t a l . , (1963). , J . Chrom.

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